| Fuel content | |
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| OELCHECK Test equipment: | Gas-phase chromatograph Clarus 500 from PerkinElmer |
| Sample quantity needed: | 3 ml |
| Unit: | % (volume) |
| Test result: | Fuel content in engine oil |
| Operating time: | ~ 5 minutes |
| Analysis of: | Oils from gasoline-, diesel- and biodiesel engines |
| Brief description: | With the help of gas-phase chromatograph, it`s possible
to separate complex mixture of materials in their components. Thereby the mixture of materials, which has to be investigated, is injected into a fine capillary column by an injector. This column is out of a material similar to glass and inside coated with chemical modified polysiloxane. The capillary column has a length of 15 m and an inner diameter of 0.25 mm. The polysiloxane layer has a thickness of only 0.25 µm. The column is mounted in a thermal adjustable oven. Hydrogen is permanent flowing through the column as carrier gas. As soon as the used engine oil gets into the column, it becomes vaporized and it`s single components are carried from the carrier gas trough the column. Depending to their structure and the oven temperature the single components are vaporizing with different speed. Therefore their resistance time at the surface of the column is different and they are going to be split according to their boiling temperature. A detector registers the single components, when they leave the column. The detector draws the single elements into a diagram. As later a component comes to the exit of the column, as higher the boiling temperature is. The area below a peak from the Gas-phase chromatograph is proportional to the amount of the component in the mixture. |
| Statement: | There are different possibilities for the fuel to come into the
motor oil. For example as condensate during cold start of the motor or as blow by
gas because of wrong adjusted carburettor. Other reasons are blocked air filters
or damaged injection nozzles. It`s also possible to find the comparatively difficult ignitable “biodiesel” as fuel in the motor oil. If there is too much fuel in the motor oil, it becomes too weak to build up a stable lubrication film. |
| Last modified: September 2010, © OELCHECK GmbH | Disclaimer Imprint |